Nanomaterials, Free Full-Text
Por um escritor misterioso
Last updated 30 julho 2024
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Due to their diverse and unique physical properties, miktoarm star copolymers (μ-SCPs) have garnered significant attention. In our study, we employed α-monobomoisobutyryl-terminated polydimethylsiloxane (PDMS-Br) to carry out styrenics-assisted atom transfer radical coupling (SA ATRC) in the presence of 4-vinylbenzyl alcohol (VBA) at 0 °C. By achieving high coupling efficiency (χc = 0.95), we obtained mid-chain functionalized PDMS-VBAm-PDMS polymers with benzylic alcohols. Interestingly, matrix-assisted laser desorption/ionization time of flight mass spectrometry (MALDI-TOF MS) analysis revealed the insertion of only two VBA coupling agents (m = 2). Subsequently, the PDMS-VBA2-PDMS products underwent mid-chain extensions using ε-caprolactone (ε-CL) through ring-opening polymerization (ROP) with an efficient organo-catalyst at 40 °C, resulting in the synthesis of novel (PDMS)2-μ-(PCL)2 μ-SCPs. Eventually, novel (PDMS)2-μ-(PCL)2 μ-SCPs were obtained. The obtained PDMS-μ-PCL μ-SCPs were further subjected to examination of their solid-state self-assembly through small-angle X-ray scattering (SAXS) experiments. Notably, various nanostructures, including lamellae and hexagonally packed cylinders, were observed with a periodic size of approximately 15 nm. As a result, we successfully developed a simple and effective reaction combination (Є) strategy (i.e., SA ATRC-Є-ROP) for the synthesis of well-defined PDMS-μ-PCL μ-SCPs. This approach may open up new possibilities for fabricating nanostructures from siloxane-based materials.
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Frontiers The Application of Nanotechnology for the Diagnosis and Treatment of Brain Diseases and Disorders
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Biogenic Synthesis of Metallic Nanoparticles by Plant Extracts
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Tribology of carbon nanotubes - About Tribology
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PDF] Nanomaterials and nanoparticles: Sources and toxicity
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Nanomaterials, Free Full-Text
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Journal of Nanotechnology Free Open Access Journals
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Nanoparticle - Wikipedia
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Agriculture nanotechnology: Translating research outcome to field applications by influencing environmental sustainability - ScienceDirect
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Proceedings of the Institution of Mechanical Engineers, Part N: Journal of Nanomaterials, Nanoengineering and Nanosystems: Sage Journals
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Frontiers Nanotechnology in Colorectal Cancer for Precision Diagnosis and Therapy
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Nanoparticle, Definition, Size Range, & Applications
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Nanomaterials: Applications, waste-handling, environmental toxicities, and future challenges – A review - ScienceDirect
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